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The experimental
equipment of the Liquid Crystal Group in Stuttgart consists of:
Polarizing
microscopy
(Olympus BH-2, Leica DM-LP) with hot stages (Mettler FP 5, Instec
HS1-i) for characterization / investigation of liquid crystalline
materials and their mesomorphism in transmission and reflection. For
microphotographs digital still and video cameras are available. The
extension of the microscopes with an optical multi-channel analyzer
(Lambda LS-200) allows the determination of the helical pitch through
measurement of the selective reflection wavelength of chiral liquid
crystal samples with helicoidal superstructure.
X-ray laboratory
for structural investigations of liquid crystalline materials,
consisting of an X-ray generator (Siemens, Cu-Kα,
λ = 1.5418
Å,
Ni-filter), flat camera and ‘Imaging plate’ 2D-detector system (Fuji
BAS 3000) for investigations of wide angle X-ray scattering (WAXS) of
samples aligned in a magnetic field. A high-accuracy temperature
controller (Lake-Shore control system, rt. to 200°C), a Kratky compact
camera (A. Paar) with sample temperature control and an electronic
1D-detector (M. Braun) for investigations of the small angle X-ray
scattering (SAXS) are also available.
Additionally, a Bruker
AXS NanoSTAR device for investigations of wide and small angle X-ray
scattering, equipped with a temperature control unit, magnetic field
for sample alignment and two-dimensional detector. The special setup
of the NanoSTAR allows for SAXS-investigations of periodicities
ranging from 1 nm to 100 nm.
Chemical laboratory
with basic equipment for synthesis and purification as well as sample
preparation.
Optical laboratory
with a vibration-damped optical table and basic opto-mechanical
equipment for construction of various optical and electro-optical
experiments on liquid crystals, e.g. pitch measurements by laser light
diffraction or tilt- and birefringence measurements with a rotating
analyzer.
Research electromagnet
(Bruker B-E 25) for reorientation experiments on liquid crystal
samples.
Electro-optics setup,
consisting of a polarizing microscope with hot stage, waveform
generator, power amplifier, photo detector, measuring amplifier and a
digital storage oscilloscope, for studies of electro-optical effects
in liquid crystals.
Dielectric spectroscopy setup
(5 Hz - 1
GHz) consisting of a low-frequency impedance analyzer (Hewlett Packard
HP 4192A, 5 Hz - 13 MHz), a radio-frequency reflectometer (Hewlett
Packard HP 4291B, 1 MHz - 1 GHz), various measuring cells, a sample
temperature controller (Novocontrol, Novotherm) as well as control-
and analysis software for investigations
of
the dielectric
properties / relaxations in liquid crystal materials.
More details here.
Polarimeter (Perkin-Elmer
241 MC) for measuring the optical rotation dispersion (ORD), e.g. for
determination of handedness and pitch of chiral liquid crystals with a
helicoidal superstructure.
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